Process monitoring, using methods from system identification and chemometrics

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Event details

Date 26.02.2010
Hour 10:15
Speaker Prof. R.Ergon - Telemark University College, Norway
Location
ME C2 405
Category Conferences - Seminars
On-line measurements of product qualities (primary outputs y) from industrial processes (chemical plants, food industry, etc.) are often not feasible. Instead, samples are taken at more or less regular intervals and brought to the laboratory for costly and time-consuming analyses. There is thus a need for primary output estimation at a high sampling rate, based on known inputs u and secondary process measurements z (flows, temperatures, etc.). In my talk I will discuss several related aspects of this: For dynamical systems, we may use Kalman filtering and system identification methods, also when the primary samples are obtained at a very low and irregular sampling rate. Spectral secondary measurements (NIR, acoustics, etc.) must then be compressed into principal components, using principal component or least squares regression (PCR/PLSR). The estimates of y may also be used in, e.g., Smidt controller feedback structures. PCR and PLSR may also be used directly for primary output estimation, using statistical limits for normal process operation. The Hotelling's T2 statistic is then used to see if new z samples are acceptably close to the normal operating point within the projection space, while the squared prediction error SPE or Q statistic is used to detect abnormal deviations outside of the projection space. For this purpose new samples are split into z = zmodel + e, and for PCR this is unproblematic. The corresponding splitting in PLSR is much discussed at the time, and the issue is also complicated by sampling errors in y, which are often larger than errors in z. The splitting of z in PLSR, i.e. the definition of zmodel and e, also affects the score-loading correspondence, and is thus of interest for fault diagnosis methods.

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  • General public
  • Free

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